Clonal selection and in vivo quantitation of protein interactions with protein-fragment complementation assays

Proc Natl Acad Sci U S A. 1999 May 11;96(10):5394-9. doi: 10.1073/pnas.96.10.5394.

Abstract

Two strategies are described for detecting constitutive or induced protein-protein interactions in intact mammalian cells; these strategies are based on oligomerization domain-assisted complementation of rationally designed fragments of the murine enzyme dihydrofolate reductase (DHFR; EC 1.5.1.3). We describe a dominant clonal-selection assay of stably transfected cells expressing partner proteins FKBP (FK506 binding protein) and FRAP (FKBP-rapamycin binding protein) fused to DHFR fragments and show a rapamycin dose-dependent survival of clones that requires approximately 25 molecules of reconstituted DHFR per cell. A fluorescence assay also is described, based on stoichiometric binding of fluorescein-methotrexate to reconstituted DHFR in vivo. Formation of the FKBP-rapamycin-FRAP complex is detected in stably and transiently transfected cells. Quantitative rapamycin dose-dependence of this complex is shown to be consistent with in vitro binding and distinguishable from a known constitutive interaction of FKBP and FRAP. We also show that this strategy can be applied to study membrane protein receptors, demonstrating dose-dependent activation of the erythropoietin receptor by ligands. The combination of these clonal-selection and fluorescence assays in intact mammalian cells makes possible selection by simple survival, flow cytometry, or both. High-throughput drug screening and quantitative analysis of induction or disruption of protein-protein interactions are also made possible.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • CHO Cells
  • Carrier Proteins*
  • Cell Survival
  • Cricetinae
  • Erythropoietin / pharmacology
  • Flow Cytometry
  • Fluoresceins
  • Genetic Complementation Test
  • Immunophilins / analysis*
  • Immunophilins / genetics
  • Methotrexate / analogs & derivatives
  • Mice
  • Microscopy, Fluorescence
  • Peptides, Cyclic / pharmacology
  • Phosphotransferases (Alcohol Group Acceptor)*
  • Protein Binding
  • Receptors, Erythropoietin / analysis
  • Recombinant Fusion Proteins / analysis
  • Sirolimus / pharmacology
  • TOR Serine-Threonine Kinases
  • Tacrolimus / pharmacology
  • Tacrolimus Binding Proteins
  • Tetrahydrofolate Dehydrogenase / analysis*
  • Tetrahydrofolate Dehydrogenase / genetics
  • Transfection

Substances

  • Carrier Proteins
  • EPO mimetic peptide 1
  • Fluoresceins
  • Peptides, Cyclic
  • Receptors, Erythropoietin
  • Recombinant Fusion Proteins
  • fluorescein-methotrexate
  • Erythropoietin
  • Tetrahydrofolate Dehydrogenase
  • Phosphotransferases (Alcohol Group Acceptor)
  • mTOR protein, mouse
  • TOR Serine-Threonine Kinases
  • Tacrolimus Binding Proteins
  • Immunophilins
  • Sirolimus
  • Tacrolimus
  • Methotrexate