Total synthesis of sufentanil

Arch Pharm Res. 1999 Aug;22(4):398-400. doi: 10.1007/BF02979064.

Abstract

Sufentanil, a potent anilidopiperidine analgesic, was synthesized from a simple thiophenylethylamine via six step sequence. The key parts of this synthesis involved an efficient construction of thiophenylethylpiperidone by aminomethano desilylation-cyclization followed by Swern oxidation and a direct regioselective N-nucleophilic spiral epoxide cleavage with aniline promoted by Lewis acids.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Analgesics, Opioid / chemical synthesis*
  • Analgesics, Opioid / chemistry
  • Indicators and Reagents
  • Mannich Bases
  • Spectrophotometry, Infrared
  • Sufentanil / chemical synthesis*
  • Sufentanil / chemistry

Substances

  • Analgesics, Opioid
  • Indicators and Reagents
  • Mannich Bases
  • Sufentanil