A molecular scanner to automate proteomic research and to display proteome images

Anal Chem. 1999 Nov 1;71(21):4981-8. doi: 10.1021/ac990449e.

Abstract

Identification and characterization of all proteins expressed by a genome in biological samples represent major challenges in proteomics. Today's commonly used high-throughput approaches combine two-dimensional electrophoresis (2-DE) with peptide mass fingerprinting (PMF) analysis. Although automation is often possible, a number of limitations still adversely affect the rate of protein identification and annotation in 2-DE databases: the sequential excision process of pieces of gel containing protein; the enzymatic digestion step; the interpretation of mass spectra (reliability of identifications); and the manual updating of 2-DE databases. We present a highly automated method that generates a fully annoated 2-DE map. Using a parallel process, all proteins of a 2-DE are first simultaneously digested proteolytically and electro-transferred onto a poly(vinylidene difluoride) membrane. The membrane is then directly scanned by MALDI-TOF MS. After automated protein identification from the obtained peptide mass fingerprints using PeptIdent software (http://www.expasy.ch/tools/peptident.html + ++), a fully annotated 2-D map is created on-line. It is a multidimensional representation of a proteome that contains interpreted PMF data in addition to protein identification results. This "MS-imaging" method represents a major step toward the development of a clinical molecular scanner.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Automation
  • Blood Proteins / analysis
  • Blood Proteins / chemistry
  • Electrophoresis, Gel, Two-Dimensional / methods
  • Electrophoresis, Polyacrylamide Gel / methods
  • Humans
  • Image Processing, Computer-Assisted / instrumentation
  • Image Processing, Computer-Assisted / methods*
  • Peptide Mapping / methods*
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization / methods
  • Trypsin Inhibitor, Kunitz Soybean / analysis
  • Trypsin Inhibitor, Kunitz Soybean / chemistry

Substances

  • Blood Proteins
  • Trypsin Inhibitor, Kunitz Soybean