The role of the conserved box E residues in the active site of the Escherichia coli type I signal peptidase

J Biol Chem. 2000 Mar 3;275(9):6490-8. doi: 10.1074/jbc.275.9.6490.

Abstract

Type I signal peptidases are integral membrane proteins that function to remove signal peptides from secreted and membrane proteins. These enzymes carry out catalysis using a serine/lysine dyad instead of the prototypical serine/histidine/aspartic acid triad found in most serine proteases. Site-directed scanning mutagenesis was used to obtain a qualitative assessment of which residues in the fifth conserved region, Box E, of the Escherichia coli signal peptidase I are critical for maintaining a functional enzyme. First, we find that there is no requirement for activity for a salt bridge between the invariant Asp-273 and the Arg-146 residues. In addition, we show that the conserved Ser-278 is required for optimal activity as well as conserved salt bridge partners Asp-280 and Arg-282. Finally, Gly-272 is essential for signal peptidase I activity, consistent with it being located within van der Waals proximity to Ser-278 and general base Lys-145 side-chain atoms. We propose that replacement of the hydrogen side chain of Gly-272 with a methyl group results in steric crowding, perturbation of the active site conformation, and specifically, disruption of the Ser-90/Lys-145 hydrogen bond. A refined model is proposed for the catalytic dyad mechanism of signal peptidase I in which the general base Lys-145 is positioned by Ser-278, which in turn is held in place by Asp-280.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Bacterial Outer Membrane Proteins / metabolism
  • Bacterial Proteins / chemistry
  • Binding Sites
  • Circular Dichroism
  • Electrophoresis, Polyacrylamide Gel
  • Escherichia coli / enzymology*
  • Hydrogen Bonding
  • Membrane Proteins*
  • Micrococcal Nuclease / metabolism
  • Models, Molecular
  • Mutagenesis
  • Mutation
  • Protein Conformation
  • Protein Precursors / metabolism
  • Serine Endopeptidases / chemistry*
  • Serine Endopeptidases / genetics

Substances

  • Bacterial Outer Membrane Proteins
  • Bacterial Proteins
  • Membrane Proteins
  • Protein Precursors
  • pro-OmpA nuclease A
  • Micrococcal Nuclease
  • Serine Endopeptidases
  • type I signal peptidase