The conserved RING-H2 finger of ROC1 is required for ubiquitin ligation

J Biol Chem. 2000 May 19;275(20):15432-9. doi: 10.1074/jbc.M907300199.

Abstract

ROC1 is a common component of a large family of ubiquitin E3 ligases that regulate cell cycle progression and signal transduction pathways. Here we present evidence suggesting that a conserved RING-H2 structure within ROC1 is critical for its ubiquitin ligation function. Mercury-containing sulfhydryl modification agents (rho-hydroxymercuribenzoate and mercuric chloride) irreversibly inhibit the ROC1-CUL1 ubiquitin ligase activity without disrupting the complex. Consistent with this, these reagents also eliminate the ability of the Skp1-CUL1-HOS-ROC1 E3 ligase complex to support the ubiquitination of IkappaBalpha. Site-directed mutagenesis analysis identifies RING-H2 finger residues Cys(42), Cys(45), Cys(75), His(77), His(80), Cys(83), Cys(94), and Asp(97) as being essential for the ROC1-dependent ubiquitin ligase activity. Furthermore, C42S/C45S and H80A mutations reduce the ability of ROC1 to interact with CUL1 in transfected cells and diminish the capacity of ROC1-CUL1 to form a stable complex with Cdc34 in vitro. However, C75S, H77A, C94S, and D97A substitutions have no detectable effect on ROC1 binding activities. Thus, the ROC1 RING-H2 finger may possess multiple biochemical properties that include stabilizing an interaction with CUL1 and recruiting Cdc34. A possible role of the RING finger in facilitating the Ub transfer reaction is discussed.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Amino Acid Substitution
  • Anaphase-Promoting Complex-Cyclosome
  • Animals
  • Binding Sites
  • Cell Line
  • Conserved Sequence
  • Cysteine
  • Humans
  • Hydroxymercuribenzoates / pharmacology
  • Kinetics
  • Ligases / antagonists & inhibitors
  • Ligases / chemistry*
  • Ligases / metabolism*
  • Mercuric Chloride / pharmacology
  • Mice
  • Mutagenesis, Site-Directed
  • Protein Conformation
  • Recombinant Fusion Proteins / metabolism
  • Sulfhydryl Reagents / pharmacology
  • Transfection
  • Ubiquitin-Conjugating Enzymes
  • Ubiquitin-Protein Ligase Complexes*
  • Ubiquitin-Protein Ligases
  • Ubiquitins / metabolism*

Substances

  • Hydroxymercuribenzoates
  • Recombinant Fusion Proteins
  • Sulfhydryl Reagents
  • Ubiquitins
  • 4-hydroxymercuribenzoate
  • Mercuric Chloride
  • CDC34 protein, human
  • Ubiquitin-Conjugating Enzymes
  • Ubiquitin-Protein Ligase Complexes
  • Anaphase-Promoting Complex-Cyclosome
  • Ubiquitin-Protein Ligases
  • Ligases
  • Cysteine