Mechanistic studies of radical-based processes. Use and misuse of EPR spectroscopy

Org Lett. 2000 Jun 1;2(11):1553-5. doi: 10.1021/ol005741j.

Abstract

The identification of the species observed by EPR spectroscopy in the SmI(2)-promoted coupling of N-(N', N'-dialkylaminoalkyl)benzotriazoles as substituted benzyl radicals is disputed on the basis of results obtained studying the model radical derived from tribenzylamine.