Abstract
In the course of our screening for inhibitors of sphingosine kinase, we found an active compound from a culture broth of a discomycete, Trichopezizella barbata SANK 25395. The structure of the compound, named F-12509A, was elucidated by a combination of spectroscopic analyses, to be a new sesquiterpene quinone consisting of a drimane moiety and a dihydroxybenzoquinone. Enzyme kinetic analyses showed that F-12509A inhibits sphingosine kinase activity in a competitive manner with respect to sphingosine, with a Ki value of 18 microM.
MeSH terms
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Animals
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Ascomycota / metabolism*
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Benzoquinones / chemistry
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Benzoquinones / metabolism
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Benzoquinones / pharmacology*
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Brain / drug effects
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Brain / enzymology
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Enzyme Inhibitors / chemistry
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Enzyme Inhibitors / metabolism
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Enzyme Inhibitors / pharmacology*
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Kinetics
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Liver / drug effects
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Liver / enzymology
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Male
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Microsomes / drug effects
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Microsomes / enzymology
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Phosphotransferases (Alcohol Group Acceptor) / antagonists & inhibitors*
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Rats
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Rats, Wistar
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Substrate Specificity
Substances
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Benzoquinones
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Enzyme Inhibitors
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F 12509A
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Phosphotransferases (Alcohol Group Acceptor)
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sphingosine kinase