Isolation and frontier molecular orbital investigation of bioactive quinone-methide triterpenoids from the bark of Salacia petenensis

Planta Med. 2001 Feb;67(1):65-9. doi: 10.1055/s-2001-10879.

Abstract

The crude dichloromethane bark extract of Salacia petenensis (Hippocrateaceae) from Monteverde, Costa Rica, shows antibacterial and cytotoxic activity. Bioactivity-directed separation led to the isolation of tingenone and netzahualcoyonol as the biologically active materials. Also isolated from the extract were 3-methoxyfriedel-2-en-1-one (a new natural product) and 29-hydroxyfriedelan-3-one. The structures of these compounds were elucidated on the basis of NMR spectral analysis. Molecular orbital calculations have been carried out using the semi-empirical PM3 and Hartee-Fock 3-21G ab initio techniques on the quinone-methide nortriterpenoids tingenone and netzahualcoyonol, as well as on the nucleotide bases adenine, guanine, cytosine, and thymine. The molecular orbital calculations suggest that a possible mode of cytotoxic action of quinone-methide triterpenoids involves quasi-intercalative interaction of the compounds with DNA followed by nucleophilic addition of the DNA base to carbon-6 of the triterpenoid.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Indolequinones*
  • Indoles / chemistry
  • Indoles / isolation & purification*
  • Models, Molecular
  • Molecular Structure
  • Quinones / chemistry
  • Quinones / isolation & purification*
  • Rosales / chemistry*
  • Triterpenes / chemistry
  • Triterpenes / isolation & purification*

Substances

  • Indolequinones
  • Indoles
  • Quinones
  • Triterpenes
  • quinone methide