Analysis of phenolic constituents of biological interest in red wines by high-performance liquid chromatography

J Chromatogr A. 2001 Jul 13;922(1-2):359-63. doi: 10.1016/s0021-9673(01)00913-x.

Abstract

We describe a reversed-phase HPLC method that uses gradient elution and diode array detection to determine four biologically active phenolic constituents of red wines: gallic acid, trans-resveratrol, quercetin and rutin. The method permits direct injection without sample pre-treatment. ODS Hypersil served as the stationary phase; the gradient was formed by acetic acid, methanol, and water. Each analysis required an equilibration period of 10 min and a run time of 50 min for completion. Previously, total phenols were analysed according to the Folin-Ciocalteu method, using gallic acid as the standard, and the results are given as gallic acid equivalent.

MeSH terms

  • Calibration
  • Chromatography, High Pressure Liquid / methods*
  • Phenols / analysis*
  • Spectrophotometry, Ultraviolet
  • Wine / analysis*

Substances

  • Phenols