Structure-based design and protein X-ray analysis of a protein kinase inhibitor

Bioorg Med Chem Lett. 2002 Jan 21;12(2):221-4. doi: 10.1016/s0960-894x(01)00715-6.

Abstract

A 5-aryl-1H-pyrazole molecular scaffold was designed to ligate the ATP binding site of cyclin dependent kinase 2 (CDK2) on the basis of crystallographic information. A search of the compound collection of Novartis using this scaffold as substructure query led to the identification of PKF049-365 as a representative of a new class of inhibitors of the cell cycle kinases CDK1/2. The three-dimensional structure of CDK2 in complex with PKF049-365 was subsequently determined by protein crystallography and refined to 1.53 A resolution. The X-ray analysis confirmed the binding mode expected from the design hypothesis. In addition, it revealed an alternative binding orientation involving a second tautomeric form of the inhibitor that was not envisaged during the design stage.

MeSH terms

  • Enzyme Inhibitors / chemistry
  • Enzyme Inhibitors / pharmacology*
  • Models, Molecular
  • Molecular Structure
  • Protein Kinase Inhibitors*
  • X-Ray Diffraction

Substances

  • Enzyme Inhibitors
  • Protein Kinase Inhibitors

Associated data

  • PDB/1JVP