Exploring the active site of plant glutaredoxin by site-directed mutagenesis

FEBS Lett. 2002 Jan 30;511(1-3):145-9. doi: 10.1016/s0014-5793(01)03302-6.

Abstract

Six mutants (Y26A, C27S, Y29F, Y29P, C30S and Y26W/Y29P) have been engineered in order to explore the active site of poplar glutaredoxin (Grx) (Y26CPYC30). The cysteinic mutants indicate that Cys 27 is the primary nucleophile. Phe is a good substitute for Tyr 29, but the Y29P mutant was inactive. The Y26A mutation caused a moderate loss of activity. The YCPPC and WCPPC mutations did not improve the reactivity of Grx with the chloroplastic NADP-malate dehydrogenase, a well known target of thioredoxins (Trxs). The results are discussed in relation with the known biochemical properties of Grx and Trx.

MeSH terms

  • Amino Acid Sequence
  • Amino Acids, Aromatic / genetics
  • Amino Acids, Aromatic / metabolism
  • Binding Sites
  • Dehydroascorbic Acid / metabolism
  • Dehydroascorbic Acid / pharmacology
  • Disulfides / metabolism
  • Enzyme Activation
  • Ethanol / analogs & derivatives*
  • Ethanol / metabolism
  • Glutaredoxins
  • Magnoliopsida* / genetics
  • Magnoliopsida* / metabolism
  • Malate Dehydrogenase / metabolism
  • Mutagenesis, Site-Directed / genetics*
  • NADP / metabolism
  • Oxidation-Reduction
  • Oxidoreductases*
  • Plant Proteins / chemistry
  • Plant Proteins / genetics
  • Plant Proteins / metabolism
  • Proteins / chemistry*
  • Proteins / genetics*
  • Proteins / metabolism
  • Trees / genetics
  • Trees / metabolism
  • Tyrosine / metabolism

Substances

  • Amino Acids, Aromatic
  • Disulfides
  • Glutaredoxins
  • Plant Proteins
  • Proteins
  • Ethanol
  • Tyrosine
  • 2-hydroxyethyl disulfide
  • NADP
  • Oxidoreductases
  • Malate Dehydrogenase
  • Dehydroascorbic Acid