Antifungal activity of eupolauridine and its action on DNA topoisomerases

Antimicrob Agents Chemother. 2002 Jun;46(6):1785-92. doi: 10.1128/AAC.46.6.1785-1792.2002.

Abstract

The azafluoranthene alkaloid eupolauridine has previously been shown to have in vitro antifungal activity and selective inhibition of fungal topoisomerase I. The present study was undertaken to examine further its selectivity and mode of action. Eupolauridine completely inhibits the DNA relaxation activity of purified fungal topoisomerase I at 50 microg/ml, but it does not stabilize the cleavage complex of either human or fungal topoisomerase I. Cleavage complex stabilization is the mode of action of topoisomerase I targeting drugs of the camptothecin family. Also, unlike camptothecin, eupolauridine does not cause significant cytotoxicity in mammalian cells. To determine if the inhibition of topoisomerase I is the principal mode of antifungal action of eupolauridine, Saccharomyces cerevisiae strains with alterations in topoisomerase genes were used in clonogenic assays. The antifungal activity of eupolauridine was not diminished in the absence of topoisomerase I; rather, the cells lacking the enzyme were more sensitive to the drug. Cell-killing activity of eupolauridine was also more pronounced in cells that overexpressed topoisomerase II. In vitro assays with the purified yeast enzyme confirmed that eupolauridine stabilized topoisomerase II covalent complexes. These results indicate that a major target for fungal cell killing by eupolauridine is DNA topoisomerase II rather than topoisomerase I, but does not exclude the possibility that the drug also acts against other targets.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Alkaloids / pharmacology*
  • Antifungal Agents / pharmacology*
  • Candida albicans / drug effects
  • Candida albicans / genetics
  • Catalysis
  • Cell Survival / drug effects
  • Culture Media
  • DNA, Fungal / chemistry
  • DNA, Fungal / drug effects
  • Enzyme Inhibitors / pharmacology*
  • Fluorenes*
  • Humans
  • Indenes
  • Microbial Sensitivity Tests
  • Naphthyridines
  • Saccharomyces cerevisiae / drug effects
  • Saccharomyces cerevisiae / genetics
  • Topoisomerase I Inhibitors*
  • Topoisomerase II Inhibitors
  • Tumor Cells, Cultured

Substances

  • Alkaloids
  • Antifungal Agents
  • Culture Media
  • DNA, Fungal
  • Enzyme Inhibitors
  • Fluorenes
  • Indenes
  • Naphthyridines
  • Topoisomerase I Inhibitors
  • Topoisomerase II Inhibitors
  • eupolauridine