The effect of core destabilization on the mechanical resistance of I27

Biophys J. 2002 Jul;83(1):458-72. doi: 10.1016/S0006-3495(02)75182-5.

Abstract

It is still unclear whether mechanical unfolding probes the same pathways as chemical denaturation. To address this point, we have constructed a concatamer of five mutant I27 domains (denoted (I27)(5)*) and used it for mechanical unfolding studies. This protein consists of four copies of the mutant C47S, C63S I27 and a single copy of C63S I27. These mutations severely destabilize I27 (DeltaDeltaG(UN) = 8.7 and 17.9 kJ mol(-1) for C63S I27 and C47S, C63S I27, respectively). Both mutations maintain the hydrogen bond network between the A' and G strands postulated to be the major region of mechanical resistance for I27. Measuring the speed dependence of the force required to unfold (I27)(5)* in triplicate using the atomic force microscope allowed a reliable assessment of the intrinsic unfolding rate constant of the protein to be obtained (2.0 x 10(-3) s(-1)). The rate constant of unfolding measured by chemical denaturation is over fivefold faster (1.1 x 10(-2) s(-1)), suggesting that these techniques probe different unfolding pathways. Also, by comparing the parameters obtained from the mechanical unfolding of a wild-type I27 concatamer with that of (I27)(5)*, we show that although the observed forces are considerably lower, core destabilization has little effect on determining the mechanical sensitivity of this domain.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Connectin
  • Dose-Response Relationship, Drug
  • Kinetics
  • Magnetic Resonance Spectroscopy
  • Models, Molecular
  • Molecular Sequence Data
  • Monte Carlo Method
  • Muscle Proteins / chemistry*
  • Muscle Proteins / metabolism
  • Mutation
  • Peptide Fragments / chemistry*
  • Peptide Fragments / metabolism
  • Protein Denaturation
  • Protein Folding
  • Protein Kinases / chemistry*
  • Protein Kinases / metabolism
  • Protein Structure, Secondary
  • Protein Structure, Tertiary
  • Proteins / chemistry*
  • Thermodynamics

Substances

  • Connectin
  • Muscle Proteins
  • Peptide Fragments
  • Proteins
  • Protein Kinases