Tandem intramolecular silylformylation-crotylsilylation: highly efficient synthesis of polyketide fragments

J Am Chem Soc. 2002 Jul 10;124(27):7890-1. doi: 10.1021/ja026511y.

Abstract

Polyketide fragments may be rapidly and efficiently assembled in the tandem intramolecular silylformylation-crotylsilylation of alkenes and alkynes. The reactions establish up to three new stereocenters with good-to-excellent diastereoselectivity, and the use of the reaction in an iterative sense is demonstrated. In addition, a new dihydrosilane alcoholysis reaction has been developed, leading to a highly efficient sequence.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Alcohols / chemical synthesis*
  • Polymers / chemical synthesis*
  • Silanes / chemistry*

Substances

  • Alcohols
  • Polymers
  • Silanes
  • polyol