The C-terminal segment of the 1,3-beta-glucanase Ole e 9 from olive (Olea europaea) pollen is an independent domain with allergenic activity: expression in Pichia pastoris and characterization

Biochem J. 2003 Feb 1;369(Pt 3):593-601. doi: 10.1042/BJ20020423.

Abstract

Several allergenic proteins, such as the 1,3-beta-glucanases, have been associated with plant defence responses. Ole e 9 (46 kDa) is a 1,3-beta-glucanase and major allergen from olive pollen, which is a principal cause of allergy in Mediterranean countries. Its C-terminal segment (101 amino acid residues) has been produced as a recombinant polypeptide in the yeast Pichia pastoris. The cDNA encoding the polypeptide was inserted into the plasmid vector pPICZalpha-A and overexpressed in KM71 yeast cells. The recombinant product was purified by size-exclusion chromatography followed by reversed-phase HPLC. Edman degradation, MS and CD were used to determine molecular properties of the recombinant polypeptide, which exhibited 16% alpha-helix and 30% beta-sheet as regular elements of secondary structure. Disulphide bridges of the molecule were determined at positions Cys-14-Cys-76, Cys-33-Cys-94 and Cys-39-Cys-48. The high IgE-binding capability of the recombinant C-terminal segment of Ole e 9 against sera from Ole e 9-sensitive individuals, which was determined by immunoblotting and ELISA inhibition, supported the proper folding of the polypeptide and the maintenance of antigenic properties that it exhibits as a part of the whole allergen. These data indicated that this portion of Ole e 9 constitutes an independent domain, which could be used to study its three-dimensional structure and function, as well as for clinical purposes such as diagnosis and specific immunotherapy. Since it shows sequence similarity with portions of 1,3-beta-glucanases from plant tissues and the Gas/Phr/Epd protein families involved in yeast morphogenesis, we suggest that this domain could play an equivalent functional role within these enzymes.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Allergens / chemistry
  • Allergens / genetics
  • Allergens / immunology
  • Allergens / metabolism
  • Allergens / physiology*
  • Amino Acid Sequence
  • Antigens, Plant
  • Chromatography, High Pressure Liquid
  • Circular Dichroism
  • Disulfides
  • Enzyme-Linked Immunosorbent Assay / methods
  • Gene Expression Regulation
  • Hypersensitivity / immunology
  • Immune Sera
  • Immunoblotting
  • Immunoglobulin E / metabolism
  • Molecular Sequence Data
  • Olea
  • Peptide Fragments / genetics
  • Peptide Fragments / immunology
  • Peptide Fragments / metabolism
  • Pichia / genetics*
  • Plant Proteins / chemistry
  • Plant Proteins / physiology*
  • Pollen / chemistry*
  • Pollen / genetics
  • Protein Structure, Tertiary
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Recombinant Proteins / metabolism
  • beta-Glucosidase / chemistry
  • beta-Glucosidase / physiology*

Substances

  • Allergens
  • Antigens, Plant
  • Disulfides
  • Immune Sera
  • Peptide Fragments
  • Plant Proteins
  • Recombinant Proteins
  • Immunoglobulin E
  • OLE9 protein, Olea europaea
  • beta-Glucosidase