A stable lyophilized reagent for use in a potential reference assay for quantitation of anti-D in immunoglobulin products

Biologicals. 2002 Dec;30(4):315-21. doi: 10.1006/biol.2002.0347.

Abstract

Quality control of anti-D immunoglobulins intended for in vivo clinical use requires in vitro assay of potency. A lyophilized biotinylated monoclonal anti-D (biotinylated Brad-5; 99/698) has been evaluated for its suitability to serve as a working reagent in a competitive enzyme-linked immunoassay (EIA) for anti-D quantitation. The reagent demonstrated acceptable stability in accelerated degradation tests and following reconstitution. Twelve international laboratories obtained comparable potencies for each of nine anti-D samples using 99/698 in a standardized assay procedure using erythrocytes fixed to microtitre plates. We also describe the use of trehalose for stabilization of dried erythrocyte-coated microtitre plates.

MeSH terms

  • Antibodies, Monoclonal
  • Biotin
  • Drug Stability
  • Erythrocytes
  • Freeze Drying
  • Humans
  • Immunoenzyme Techniques / methods*
  • Immunoenzyme Techniques / standards
  • Indicators and Reagents
  • Laboratories
  • Quality Control
  • Rho(D) Immune Globulin / analysis*

Substances

  • Antibodies, Monoclonal
  • Indicators and Reagents
  • Rho(D) Immune Globulin
  • Biotin