The role of hydrogen bonding via interfacial water molecules in antigen-antibody complexation. The HyHEL-10-HEL interaction

J Biol Chem. 2003 Feb 14;278(7):5410-8. doi: 10.1074/jbc.M210182200. Epub 2002 Nov 19.

Abstract

To study the role of hydrogen bonding via interfacial water molecules in protein-protein interactions, we examined the interaction between hen egg white lysozyme (HEL) and its HyHEL-10 variable domain fragment (Fv) antibody. We constructed three antibody mutants (l-Y50F, l-S91A, and l-S93A) and investigated the interactions between the mutant Fvs and HEL. Isothermal titration calorimetry indicated that the mutations significantly decreased the negative enthalpy change (8-25 kJ mol(-1)), despite some offset by a favorable entropy change. X-ray crystallography demonstrated that the complexes had nearly identical structures, including the positions of the interfacial water molecules. Taken together, the isothermal titration calorimetric and x-ray crystallographic results indicate that hydrogen bonding via interfacial water enthalpically contributes to the Fv-HEL interaction despite the partial offset because of entropy loss, suggesting that hydrogen bonding stiffens the antigen-antibody complex.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antigen-Antibody Complex / chemistry*
  • Chickens
  • Hydrogen Bonding
  • Immunoglobulin Fragments / chemistry*
  • Immunoglobulin Fragments / immunology
  • Muramidase / chemistry*
  • Muramidase / immunology
  • Water / chemistry

Substances

  • Antigen-Antibody Complex
  • Immunoglobulin Fragments
  • Water
  • Muramidase

Associated data

  • PDB/1J10
  • PDB/1J1P
  • PDB/1J1X