A new and improved method for deglycosidation of glycopeptide antibiotics exemplified with vancomycin, ristocetin, and ramoplanin

Bioorg Med Chem Lett. 2003 Mar 24;13(6):1169-73. doi: 10.1016/s0960-894x(03)00051-9.

Abstract

A general method for the deglycosidation of glycopeptide antibiotics has been developed. Treatment of vancomycin, ristocetin, and ramoplanin with anhydrous HF results in efficient cleavage of the sugars to provide the corresponding aglycons in high yield.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Anti-Bacterial Agents / chemistry*
  • Chromatography, High Pressure Liquid
  • Depsipeptides*
  • Hydrofluoric Acid
  • Indicators and Reagents
  • Peptides, Cyclic / chemistry*
  • Pyridines / chemistry
  • Ristocetin / chemistry*
  • Solvents
  • Vancomycin / chemistry*

Substances

  • Anti-Bacterial Agents
  • Depsipeptides
  • Indicators and Reagents
  • Peptides, Cyclic
  • Pyridines
  • Solvents
  • ramoplanin
  • Ristocetin
  • Vancomycin
  • pyridine
  • Hydrofluoric Acid