Site-directed fluorescence probing to dissect the calcium-dependent association between soluble tissue factor and factor VIIa domains

Biochim Biophys Acta. 2003 May 30;1648(1-2):12-6. doi: 10.1016/s1570-9639(03)00025-6.

Abstract

We have used the site-directed labeling approach to study the Ca(2+)-dependent docking of factor VIIa (FVIIa) to soluble tissue factor (sTF). Nine Ca(2+) binding sites are located in FVIIa and even though their contribution to the overall binding between TF and FVIIa has been thoroughly studied, their importance for local protein-protein interactions within the complex has not been determined. Specifically we have monitored the association of the gamma-carboxyglutamic acid (Gla), the first EGF-like (EGF1), and the protease domains (PD) of FVIIa to sTF. Our results revealed that complex formation between sTF and FVIIa during Ca(2+) titration is initiated upon Ca(2+) binding to EGF1, the domain containing the site of highest Ca(2+) affinity. Besides we showed that a Ca(2+)-loaded Gla domain is required for an optimal association of all domains of FVIIa to sTF. Ca(2+) binding to the PD seems to be of some importance for the docking of this domain to sTF.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Calcium / metabolism
  • Epidermal Growth Factor / metabolism
  • Factor VIIa / analysis*
  • Factor VIIa / chemistry
  • Factor VIIa / metabolism
  • Fluorescent Dyes
  • Molecular Probes
  • Protein Binding
  • Protein Conformation
  • Protein Structure, Tertiary
  • Thromboplastin / analysis*
  • Thromboplastin / chemistry
  • Thromboplastin / metabolism

Substances

  • Fluorescent Dyes
  • Molecular Probes
  • Epidermal Growth Factor
  • Thromboplastin
  • Factor VIIa
  • Calcium