A novel method for measuring serum ornithine carbamoyltransferase

Ann Clin Biochem. 2003 May;40(Pt 3):264-8. doi: 10.1258/000456303321610583.

Abstract

Background: Serum ornithine carbamoyltransferase is a diagnostic marker of hepatic disorders due to its localization in periportal mitochondria.

Methods: We have developed a new method for the determination of serum ornithine carbamoyltransferase. It is based on the reverse reaction of ornithine carbamoyltransferase, using ornithine-ketoacid aminotransferase, Delta(1)-pyrroline-5-carboxylate dehydrogenase and glutamate dehydrogenase, which together convert citrulline through ornithine to glutamate. The glutamate is then quantitatively measured using glutamate oxidase and Trinder's reagent.

Results: The results obtained by this method agreed well with those obtained using the diacetylmonoxime method as a gold standard [correlation coefficient (r) = 0.973 P<0.001]. The endogenous amino acids sensitive to this method in serum (glutamate, ornithine and Delta(1)-pyrroline-5-carboxylate) were eliminated by the initial futile reaction. The new method appears to be more accurate at low levels of ornithine carbamoyltransferase activity than the diacetylmonoxime method.

Conclusions: Here we report a new method for serum ornithine carbamoyl-transferase assay which might be useful for clinical diagnosis of hepatic disorders, including hepatic cancer.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biomarkers / blood
  • Citrulline / chemistry
  • Citrulline / metabolism
  • Glutamate Dehydrogenase / metabolism
  • Glutamates / chemistry
  • Glutamates / metabolism
  • Humans
  • Liver Diseases / blood
  • Ornithine / chemistry
  • Ornithine / metabolism
  • Ornithine Carbamoyltransferase / blood*
  • Ornithine Carbamoyltransferase / metabolism*
  • Ornithine-Oxo-Acid Transaminase / chemistry
  • Ornithine-Oxo-Acid Transaminase / metabolism
  • Pyrroline Carboxylate Reductases / metabolism
  • Reference Values
  • Reproducibility of Results

Substances

  • Biomarkers
  • Glutamates
  • Citrulline
  • Ornithine
  • Glutamate Dehydrogenase
  • Pyrroline Carboxylate Reductases
  • Ornithine Carbamoyltransferase
  • Ornithine-Oxo-Acid Transaminase