The Staphostatin-staphopain complex: a forward binding inhibitor in complex with its target cysteine protease

J Biol Chem. 2003 Oct 17;278(42):40959-66. doi: 10.1074/jbc.M302926200. Epub 2003 Jul 21.

Abstract

Staphostatins are the endogenous inhibitors of the major secreted cysteine proteases of Staphylococcus aureus, the staphopains. Our recent crystal structure of staphostatin B has shown that this inhibitor forms a mixed, eight-stranded beta-barrel with statistically significant similarity to lipocalins, but not to cystatins. We now present the 1.8-A crystal structure of staphostatin B in complex with an inactive mutant of its target protease. The complex is held together through extensive interactions and buries a total surface area of 2300 A2. Unexpectedly for a cysteine protease inhibitor, staphostatin B binds to staphopain B in an almost substrate-like manner. The inhibitor polypeptide chain runs through the protease active site cleft in the forward direction, with residues IG-TS in P2 to P2' positions. Both in the free and complexed forms, the P1 glycine residue of the inhibitor is in a main chain conformation only accessible to glycines. Mutations in this residue lead to a loss of affinity of the inhibitor for protease and convert the inhibitor into a substrate.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins*
  • Carrier Proteins / chemistry*
  • Carrier Proteins / pharmacology
  • Cysteine Endopeptidases / chemistry*
  • Cysteine Endopeptidases / pharmacology
  • Dose-Response Relationship, Drug
  • Escherichia coli / metabolism
  • Humans
  • Intracellular Signaling Peptides and Proteins
  • Kinetics
  • Models, Molecular
  • Mutation
  • Peptides / chemistry
  • Protein Binding
  • Protein Conformation
  • Protein Structure, Secondary
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization
  • Time Factors

Substances

  • Bacterial Proteins
  • Carrier Proteins
  • Intracellular Signaling Peptides and Proteins
  • Peptides
  • staphostatin B protein, Staphylococcus aureus
  • Cysteine Endopeptidases
  • staphopain B protein, Staphylococcus aureus

Associated data

  • PDB/1PXV