Enantioselective syntheses and cytotoxicity of N,O-nucleosides

J Med Chem. 2003 Aug 14;46(17):3696-702. doi: 10.1021/jm0308186.

Abstract

Enantiomers of 4'-aza-2',3'-dideoxynucleosides have been prepared by two different synthetic approaches, on the basis of 1,3-dipolar cycloaddition of a chiral nitrone. Cytotoxicity and apoptotic activity have been investigated. (5'S)-5-Fluoro-1-isoxazolidin-5-yl-1H-pyrimidine-2,4-dione [(-)-AdFU], while showing low level of cytotoxicity, is a good inductor of apoptosis on lymphoid and monocytoid cells, acting as a strong potentiator of Fas-induced cell death.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antineoplastic Agents / chemical synthesis
  • Antineoplastic Agents / pharmacology
  • Antineoplastic Agents / toxicity
  • Antiviral Agents / chemical synthesis
  • Antiviral Agents / pharmacology
  • Antiviral Agents / toxicity
  • Apoptosis
  • Caspase 3
  • Caspase 8
  • Caspase 9
  • Caspase Inhibitors
  • Caspases / metabolism
  • Cell Line
  • Dideoxynucleosides / chemical synthesis*
  • Dideoxynucleosides / pharmacology
  • Dideoxynucleosides / toxicity
  • Humans
  • Isoxazoles / chemical synthesis*
  • Isoxazoles / pharmacology
  • Isoxazoles / toxicity
  • Lymphoid Tissue / cytology
  • Molecular Conformation
  • Monocytes / cytology
  • Quantum Theory
  • Stereoisomerism
  • Structure-Activity Relationship
  • Tumor Cells, Cultured
  • Uridine / analogs & derivatives
  • Uridine / chemical synthesis*
  • Uridine / pharmacology
  • Uridine / toxicity
  • fas Receptor / physiology

Substances

  • 5-fluoro-1-isoxazolidin-5-yl-1H-pyrimidine-2,4-dione
  • Antineoplastic Agents
  • Antiviral Agents
  • Caspase Inhibitors
  • Dideoxynucleosides
  • Isoxazoles
  • fas Receptor
  • CASP3 protein, human
  • CASP8 protein, human
  • CASP9 protein, human
  • Caspase 3
  • Caspase 8
  • Caspase 9
  • Caspases
  • Uridine