beta-Isocupreidine-catalyzed asymmetric Baylis-Hillman reaction of imines

Org Lett. 2003 Aug 21;5(17):3103-5. doi: 10.1021/ol035102j.

Abstract

[reaction: see text] beta-Isocupreidine (beta-ICD)-catalyzed asymmetric Baylis-Hillman reactions of aromatic imines with 1,1,1,3,3,3-hexafluoroisopropyl acrylate (HFIPA) give (S)-enriched N-protected-alpha-methylene-beta-amino acid esters. In contrast to the corresponding aldehydes, imines show the opposite enantioselectivity. A mechanistic proposal governed by hydrogen bonding is presented.