Auracyanin B structure in space group P6(5)

Acta Crystallogr D Biol Crystallogr. 2003 Sep;59(Pt 9):1545-50. doi: 10.1107/s0907444903014161. Epub 2003 Aug 19.

Abstract

The structure of auracyanin B, a 'blue' copper protein produced by Chloroflexus aurantiacus, has previously been solved and refined in the hexagonal space group P6(4)22 with a single molecule in the asymmetric unit. The protein has now been crystallized in space group P6(5), with unit-cell parameters a = b = 115.9, c = 108.2 A. In the new crystal form, the asymmetric unit contains four protein molecules. The structure has been solved by molecular replacement and refined at 1.9 A resolution. The final residuals are R = 19.2% and R(free) = 21.9%. In relation to the earlier crystal structure, the doubling of the unit-cell volume and the lower symmetry are explained by small rotations of the molecules with respect to one another.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Bacterial Proteins / chemistry*
  • Chloroflexus / chemistry
  • Crystallization
  • Crystallography, X-Ray
  • Metalloproteins / chemistry*
  • Molecular Structure

Substances

  • Bacterial Proteins
  • Metalloproteins
  • auracyanin B-1 protein, bacteria