Oltipraz inhibits 3-methylcholanthrene induction of CYP1A1 by CCAAT/enhancer-binding protein activation

J Biol Chem. 2003 Nov 7;278(45):44103-12. doi: 10.1074/jbc.M307597200. Epub 2003 Aug 26.

Abstract

Oltipraz, a cancer chemopreventive agent, induces CYP1A1 to a certain extent by transactivation of the gene via the Ah receptor (AhR)-xenobiotic response element (XRE) pathway. Previously, we showed that oltipraz promoted CCAAT/enhancer binding proteinbeta (C/EBPbeta) activation, which leads to the induction of glutathione S-transferase. Given that oltipraz activates C/EBPbeta for gene transactivation and that the putative C/EBP binding site is located in the CYP1A1 promoter region, this study investigated the effect of oltipraz on CYP1A1 induction by 3-methylcholanthrene (3-MC). 3-MC induced CYP1A1 in H4IIE cells in a time- and concentration-dependent manner. Gel shift analysis showed that 3-MC increased the band intensity of protein binding to the XRE. Immunocompetition analysis verified the specificity of AhR-XRE binding. Oltipraz (30 microM) induced CYP1A1 and the CYP1A1 promoter-luciferase gene and increased AhR DNA binding activity, which was 10-20% of those in 3-MC (100 nM)-treated cells. However, AhR-XRE binding was not increased after 10 microM oltipraz treatment. Oltipraz (10 microM) significantly inhibited CYP1A1 and CYP1A1-luciferase gene induction by 3-MC with no increase in AhR DNA binding. Oltipraz enhanced protein binding to the C/EBP binding site in the gene promoter and the binding complex comprised of C/EBPbeta and partly C/EBPdelta. Overexpression of dominant-negative mutant C/EBP significantly abolished the ability of oltipraz to suppress 3-MC-inducible CYP1A1 and the CYP1A1 reporter gene expression. Consistently, C/EBPbeta overexpression blocked CYP1A1 reporter gene induction by 3-MC. These results provide evidence that oltipraz suppresses 3-MC induction of CYP1A1 gene expression and that activation of C/EBPbeta by oltipraz contributes to suppression of 3-MC-inducible AhR-mediated CYP1A1 expression.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anticarcinogenic Agents / pharmacology*
  • Binding Sites
  • Blotting, Western
  • CCAAT-Enhancer-Binding Proteins / drug effects*
  • CCAAT-Enhancer-Binding Proteins / genetics
  • CCAAT-Enhancer-Binding Proteins / metabolism
  • Cell Line
  • Cytochrome P-450 CYP1A1 / biosynthesis*
  • Cytochrome P-450 CYP1A1 / genetics
  • DNA / metabolism
  • Gene Expression / drug effects
  • Genes, Reporter
  • Hepatocytes
  • Luciferases / genetics
  • Methylcholanthrene / pharmacology*
  • Mutation
  • Promoter Regions, Genetic / genetics
  • Pyrazines / pharmacology*
  • Rats
  • Receptors, Aryl Hydrocarbon / genetics
  • Recombinant Fusion Proteins
  • Thiones
  • Thiophenes
  • Transcriptional Activation / drug effects
  • Transfection

Substances

  • Anticarcinogenic Agents
  • CCAAT-Enhancer-Binding Proteins
  • Pyrazines
  • Receptors, Aryl Hydrocarbon
  • Recombinant Fusion Proteins
  • Thiones
  • Thiophenes
  • Methylcholanthrene
  • oltipraz
  • DNA
  • Luciferases
  • Cytochrome P-450 CYP1A1