Stable and controlled amphoteric doping by encapsulation of organic molecules inside carbon nanotubes

Nat Mater. 2003 Oct;2(10):683-8. doi: 10.1038/nmat976. Epub 2003 Sep 7.

Abstract

Single-walled carbon nanotubes (SWNTs) have strong potential for molecular electronics, owing to their unique structural and electronic properties. However, various outstanding issues still need to be resolved before SWNT-based devices can be made. In particular, large-scale, air-stable and controlled doping is highly desirable. Here we present a method for integrating organic molecules into SWNTs that promises to push the performance limit of these materials for molecular electronics. Reaction of SWNTs with molecules having large electron affinity and small ionization energy achieved p- and n-type doping, respectively. Optical characterization revealed that charge transfer between SWNTs and molecules starts at certain critical energies. X-ray diffraction experiments revealed that molecules are predominantly encapsulated inside SWNTs, resulting in an improved stability in air. The simplicity of the synthetic process offers a viable route for the large-scale production of SWNTs with controlled doping states.

Publication types

  • Evaluation Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Coated Materials, Biocompatible / chemical synthesis*
  • Coated Materials, Biocompatible / chemistry
  • Crystallization / methods*
  • Crystallography / methods*
  • Equipment Design
  • Hydrogen-Ion Concentration
  • Macromolecular Substances
  • Materials Testing
  • Molecular Conformation
  • Nanotechnology / instrumentation
  • Nanotechnology / methods*
  • Nanotubes, Carbon / chemistry*
  • Organic Chemicals / chemical synthesis
  • Organic Chemicals / chemistry*
  • Semiconductors

Substances

  • Coated Materials, Biocompatible
  • Macromolecular Substances
  • Nanotubes, Carbon
  • Organic Chemicals