Preclinical evaluation of cathepsin-degradable peptide linkers for radioimmunoconjugates

Clin Cancer Res. 2003 Sep 1;9(10 Pt 2):3865S-72S.

Abstract

Purpose: Immunoglobulins are catabolized in the hepatocytes, primarily by cathepsins. The liver becomes the likely dose-limiting tissue for radiometals, like (90)Y, in radioimmunoconjugates (RICs) used for radioimmunotherapy in combination with bone marrow support. To assess whether in vitro cathepsin-degradable peptide linkers between the chelated radiometal and the antibody decreased hepatic radiation dose, cumulated activity was used as a surrogate for radiation dose.

Experimental design: Four different cathepsin-degradable peptides used to link 1,4,7,10-tetraazacyclododecane-N,N',N",N"'-tetraacetic acid-chelated (111)In to two different monoclonal antibodies were studied in athymic mouse models of human breast cancer or lymphoma. Measured concentrations of activity during 5 days were used to reflect pharmacokinetic behavior for normal tissues and tumor. With the use of linear regression to fit a monoexponential decay function, cumulated activities in the liver and xenografts were calculated.

Results: The pharmacokinetic behavior of the cathepsin-degradable peptide-linked RICs was similar to that for the 2-iminothiolane (2IT) nondegradable linked RICs except for the liver. The liver cumulated activities of peptide-linked RICs were significantly decreased from those of the corresponding 2IT-linked RICs, varying between reductions of 59 and 68%. Cumulated activities of peptide-linked RICs in the xenografts were as great as those of 2IT RICs, so that the therapeutic indices (tumor: liver cumulated activity ratios) were substantially better for cathepsin-degradable peptide-linked RICs.

Conclusions: Cathepsin-degradable peptides used to link chelated radiometals to antibodies reduce liver radiation dose and improve the therapeutic index for radioimmunotherapy given in combination with bone marrow support.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Animals
  • Antibodies, Monoclonal / chemistry
  • Breast Neoplasms / pathology
  • Cathepsins / chemistry*
  • Chelating Agents / pharmacology
  • Chromatography, High Pressure Liquid
  • Heterocyclic Compounds, 1-Ring / pharmacology
  • Humans
  • Immunoconjugates / chemistry*
  • Indium Radioisotopes / pharmacokinetics
  • Linear Models
  • Liver / drug effects
  • Liver / metabolism
  • Liver / radiation effects*
  • Lymphoma / pathology
  • Mice
  • Mice, Nude
  • Models, Chemical
  • Neoplasm Transplantation
  • Peptides / chemistry
  • Radioimmunotherapy / methods
  • Time Factors

Substances

  • Antibodies, Monoclonal
  • Chelating Agents
  • Heterocyclic Compounds, 1-Ring
  • Immunoconjugates
  • Indium Radioisotopes
  • Peptides
  • 1,4,7,10-tetraazacyclododecane- 1,4,7,10-tetraacetic acid
  • Cathepsins