Saturation transfer difference NMR and computational modeling of a sialoadhesin-sialyl lactose complex

Carbohydr Res. 2004 Jan 22;339(2):259-67. doi: 10.1016/j.carres.2003.09.021.

Abstract

The siglecs are a family of I-type lectins binding to sialic acids on the cell surface. Sialoadhesin (siglec-1) is expressed at much higher levels in inflammatory macrophages and specifically binds to alpha-2,3-sialylated N-acetyl lactosamine residues of glycan chains. The terminal disaccharide alpha-D-Neu5Ac-(2-->3)-beta-D-Gal is thought to be the main epitope recognized by sialoadhesin. To understand the basis of this biological recognition reaction we combined NMR experiments with a molecular modeling study. We employed saturation transfer difference (STD) NMR experiments to characterize the binding epitope of alpha-2,3-sialylated lactose, alpha-D-Neu5Ac-(2-->3)-beta-D-Gal-(1-->4)-D-Glc 1 to sialoadhesin at atomic resolution. The experimental results were compared to a computational docking model and to X-ray data of a complex of sialyl lactose and sialoadhesin. The data reveal that sialoadhesin mainly recognizes the N-acetyl neuraminic acid and a small part of the galactose moiety of 1. The crystal structure of a complex of sialoadhesin with sialyl lactose 1 was used as a basis for a modeling study using the FlexiDock algorithm. The model generated was very similar to the original crystal structure. Therefore, the X-ray data were used to predict theoretical STD values utilizing the CORCEMA-STD protocol. The good agreement between experimental and theoretical STD values indicates that a combined modeling/STD NMR approach yields a reliable structural model for the complex of sialoadhesin with alpha-D-Neu5Ac-(2-->3)-beta-D-Gal-(1-->4)-D-Glc 1 in aqueous solution.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Carbohydrate Sequence
  • Computer Simulation*
  • Lactose / analogs & derivatives*
  • Lactose / chemistry*
  • Lactose / metabolism*
  • Magnetic Resonance Spectroscopy
  • Membrane Glycoproteins / chemistry*
  • Membrane Glycoproteins / metabolism*
  • Models, Molecular
  • Molecular Conformation
  • Molecular Sequence Data
  • Protein Binding
  • Receptors, Immunologic / chemistry*
  • Receptors, Immunologic / metabolism*
  • Sialic Acid Binding Ig-like Lectin 1
  • Sialic Acids / chemistry*
  • Sialic Acids / metabolism*

Substances

  • Membrane Glycoproteins
  • Receptors, Immunologic
  • Sialic Acid Binding Ig-like Lectin 1
  • Sialic Acids
  • N-acetylneuraminoyllactose
  • Lactose