Crystal structures of monoamine oxidase B in complex with four inhibitors of the N-propargylaminoindan class

J Med Chem. 2004 Mar 25;47(7):1767-74. doi: 10.1021/jm031087c.

Abstract

Monoamine oxidase B (MAO B) is an outer mitochondrial membrane enzyme that catalyzes the oxidation of arylalkylamine neurotransmitters. The crystal structures of MAO B in complex with four of the N-propargylaminoindan class of MAO covalent inhibitors (rasagiline, N-propargyl-1(S)-aminoindan, 6-hydroxy-N-propargyl-1(R)-aminoindan, and N-methyl-N-propargyl-1(R)-aminoindan) have been determined at a resolution of better than 2.1 A. Rasagiline, 6-hydroxy-N-propargyl-1(R)-aminoindan, and N-methyl-N-propargyl-1(R)-aminoindan adopt essentially the same conformation with the extended propargyl chain covalently bound to the flavin and the indan ring located in the rear of the substrate cavity. N-Propargyl-1(S)-aminoindan binds with the indan ring in a flipped conformation with respect to the other inhibitors, which causes a slight movement of the Tyr326 side chain. Four ordered water molecules are an integral part of the active site and establish H-bond interactions to the inhibitor atoms. These structural studies may guide future drug design to improve selectivity and efficacy by introducing appropriate substituents on the rasagiline molecular scaffold.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Alkynes / chemistry*
  • Binding Sites
  • Crystallography, X-Ray
  • Indans / chemistry*
  • Kinetics
  • Models, Molecular
  • Molecular Structure
  • Monoamine Oxidase / chemistry*
  • Monoamine Oxidase Inhibitors / chemistry*
  • Stereoisomerism
  • Structure-Activity Relationship

Substances

  • Alkynes
  • Indans
  • Monoamine Oxidase Inhibitors
  • rasagiline
  • Monoamine Oxidase

Associated data

  • PDB/1S2Q
  • PDB/1S2Y
  • PDB/1S3B
  • PDB/1S3E