Catalytic asymmetric synthesis of a nitrogen analogue of dialkyl tartrate by direct mannich reaction under phase-transfer conditions

Org Lett. 2004 Jul 8;6(14):2397-9. doi: 10.1021/ol049215u.

Abstract

[reaction: see text] Phase-transfer-catalyzed direct Mannich reaction of glycinate Schiff base 3 with alpha-imino ester 4 has been accomplished with high enantioselectivity by the utilization of N-spiro C(2)-symmetric chiral quaternary ammonium bromide 2 as a catalyst. This methodology enables the catalytic asymmetric synthesis of differentially protected 3-aminoaspartate, a nitrogen analogue of dialkyl tartrate. The product (syn-5) was converted into a precursor (6) of streptolidine lactam.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkanes / chemical synthesis*
  • Catalysis
  • Glycine / analogs & derivatives
  • Glycine / chemistry
  • Indicators and Reagents
  • Molecular Structure
  • Nitrogen / chemistry*
  • Stereoisomerism
  • Tartrates / chemical synthesis*

Substances

  • Alkanes
  • Indicators and Reagents
  • Tartrates
  • Nitrogen
  • Glycine