Synthesis and structure of an unexpected platinum pi complex formed from substituted 1,4-diamino ligands through an elimination process

Chemistry. 2005 Mar 18;11(7):2130-4. doi: 10.1002/chem.200401228.

Abstract

An unusual reactivity of cis-1,2-bis[(N,N-dimethylamino)methyl] cyclohexane with PtCl(2) was observed, resulting in the formation of a platinum(II) pi-olefin complex instead of the conventional square-planar cis Pt(II) coordination complex with the diamino ligand. This behavior was interpreted on the basis of the steric hindrance of the dimethylamino groups whose electron lone pairs are barely accessible to a platinum atom, which can make it difficult for both dimethylamino groups to bind platinum at the same time. This complex has been physically and spectroscopically characterized and its structure has been confirmed by using X-ray diffraction analyses on single crystals.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Crystallography, X-Ray
  • Cyclohexanes / chemistry
  • Ligands
  • Magnetic Resonance Spectroscopy / methods
  • Magnetic Resonance Spectroscopy / standards
  • Models, Molecular
  • Molecular Conformation
  • Organoplatinum Compounds / chemical synthesis*
  • Organoplatinum Compounds / chemistry*
  • Reference Standards
  • Sensitivity and Specificity

Substances

  • Cyclohexanes
  • Ligands
  • Organoplatinum Compounds
  • cis-1,2-bis((N,N-dimethylamino)methyl) cyclohexane