Simple automated preparation of O-[11C]methyl-l-tyrosine for routine clinical use

Appl Radiat Isot. 2005 Jul;63(1):55-61. doi: 10.1016/j.apradiso.2005.01.014. Epub 2005 Mar 23.

Abstract

The previously reported preparation of O-[(11)C]methyl-l-tyrosine ([(11)C]MT), a promising tumor imaging agent, has been now considerably simplified and automated. Main changes were the use of [(11)C]methyl iodide ([(11)C]MeI) in the reaction with l-tyrosine disodium and the use of solid phase extraction on commercially available cartridges instead of HPLC for the final purification. An injectable saline solution of [(11)C]MT was obtained within 30 min after EOB with radiochemical yield of ca. 60% (decay-corrected, based on [(11)C]MeI). Radiochemical purity was over 97%. The automated preparation was carried out using a miniature module employing manifold valves.

MeSH terms

  • Automation
  • Carbon Radioisotopes*
  • Chromatography, High Pressure Liquid
  • Methyltyrosines*
  • Radiopharmaceuticals*

Substances

  • Carbon Radioisotopes
  • Methyltyrosines
  • Radiopharmaceuticals