Two-stage affinity purification for inducibly phosphorylated membrane proteins

Proteomics. 2005 Jun;5(9):2417-21. doi: 10.1002/pmic.200401176.

Abstract

Characterisation of tyrosine phosphorylations induced in immune cells in response to inflammatory stimuli may help elucidate the molecular bases of the diversity of immune responses. We have used anti-phosphotyrosine antibodies in combination with cell surface biotinylation in a two-step affinity purification procedure to recover pervanadate-induced tyrosine phosphorylated proteins from sub-cellular compartments, including the cell surface, of murine T cells and macrophages prior to separation by solution-phase isoelectric focussing and one-dimensional gel electrophoresis and identification by tandem mass spectrometry.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antibodies
  • Biotinylation
  • Cell Compartmentation
  • Cell Line
  • Electrophoresis, Polyacrylamide Gel
  • Hybridomas / metabolism
  • Immunoprecipitation
  • Isoelectric Focusing
  • Macrophages / metabolism
  • Mass Spectrometry
  • Membrane Proteins / isolation & purification*
  • Membrane Proteins / metabolism
  • Mice
  • Phosphoproteins / isolation & purification*
  • Phosphoproteins / metabolism
  • Phosphorylation
  • Phosphotyrosine / immunology
  • Phosphotyrosine / metabolism
  • Protein Tyrosine Phosphatases / antagonists & inhibitors
  • Proteome / metabolism*
  • T-Lymphocytes / metabolism
  • Vanadates / pharmacology

Substances

  • Antibodies
  • Membrane Proteins
  • Phosphoproteins
  • Proteome
  • pervanadate
  • Phosphotyrosine
  • Vanadates
  • Protein Tyrosine Phosphatases