Synthesis of the spirocyclic core of the prunolides using a singlet oxygen-mediated cascade sequence

Org Lett. 2005 Jun 9;7(12):2357-9. doi: 10.1021/ol050619b.

Abstract

[reaction: see text] A highly efficient and rapid four-step synthesis of the bis-spiroketal core of the prunolide natural products, starting from furan itself, is described. The key step and culmination of the synthesis, responsible for zipping up the spirocyclic core, is a singlet oxygen-orchestrated cascade sequence in which a double photooxygenation of a 1,2-difuryl alkene precursor precedes dehydration and spirocyclization to furnish the intact prunolide core.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cyclization
  • Furans / chemical synthesis*
  • Marine Toxins / chemical synthesis*
  • Molecular Structure
  • Singlet Oxygen / chemistry*
  • Spiro Compounds / chemical synthesis*

Substances

  • Furans
  • Marine Toxins
  • Spiro Compounds
  • prunolide A
  • prunolide B
  • prunolide C
  • rubrolide A
  • Singlet Oxygen