The solution structure of a transient photoreceptor intermediate: Delta25 photoactive yellow protein

Structure. 2005 Jul;13(7):953-62. doi: 10.1016/j.str.2005.04.017.

Abstract

The N-terminally truncated variant of photoactive yellow protein (Delta25-PYP) undergoes a very similar photocycle as the corresponding wild-type protein (WT-PYP), although the lifetime of its light-illuminated (pB) state is much longer. This has allowed determination of the structure of both its dark- (pG) as well as its pB-state in solution by nuclear magnetic resonance (NMR) spectroscopy. The pG structure shows a well-defined fold, similar to WT-PYP and the X-ray structure of the pG state of Delta25-PYP. In the long-lived photocycle intermediate pB, the central beta sheet is still intact, as well as a small part of one alpha helix. The remainder of pB is unfolded and highly flexible, as evidenced by results from proton-deuterium exchange and NMR relaxation studies. Thus, the partially unfolded nature of the presumed signaling state of PYP in solution, as suggested previously, has now been structurally demonstrated.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / genetics*
  • Crystallography, X-Ray
  • Halorhodospira halophila / metabolism
  • Light
  • Magnetic Resonance Spectroscopy
  • Models, Chemical
  • Models, Molecular
  • Models, Statistical
  • Photoreceptors, Microbial / chemistry*
  • Photoreceptors, Microbial / genetics*
  • Protein Conformation
  • Protein Folding
  • Protein Structure, Tertiary
  • Protons
  • Signal Transduction
  • X-Rays

Substances

  • Bacterial Proteins
  • Photoreceptors, Microbial
  • Protons
  • photoactive yellow protein, Bacteria