Resonantly enhanced off-specular X-ray scattering from polymer/polymer interfaces

Eur Phys J E Soft Matter. 2005 Jul;17(3):353-9. doi: 10.1140/epje/i2004-10147-4. Epub 2005 Jul 18.

Abstract

We have used measurements of the absolute intensity of diffuse X-ray scattering to extract the interfacial tension of a buried polymer/polymer interface. Diffuse scattering was excited by an X-ray standing wave whose phase was adjusted to have a high intensity at the polymer/polymer interface and simultaneously a node at the polymer/air interface. This method permits the capillary-wave-induced roughness of the interface, and hence the interfacial tension, to be measured independently of the polymer/polymer interdiffusion.

Publication types

  • Evaluation Study
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Algorithms*
  • Computer Simulation
  • Models, Chemical*
  • Models, Molecular*
  • Polystyrenes / analysis
  • Polystyrenes / chemistry*
  • Refractometry / methods*
  • Scattering, Radiation
  • Surface Properties
  • X-Ray Diffraction / methods*

Substances

  • Polystyrenes