[Synthesis of purpure-18-imide and study on its interaction with bovine serum albumins by fluorescence]

Guang Pu Xue Yu Guang Pu Fen Xi. 2005 Apr;25(4):594-7.
[Article in Chinese]

Abstract

Purpure-18-imide was synthesized based on the porphyrin's special affinity for cancer cells and the antitumor activity of pyrrolidine compound. The binding reaction between purpure-18-imide and bovine serum albumins (BSA) in aqueous was studied by fluorescence and UV-Vis absorption spectra. The research results indicated that the combination reaction of them was a single static quenching process. In aqueous, purpure-18-imide strongly bound BSA with molar ratio of 1:1. The binding constant K0 was 5.386 x 10(5) L x mol(-1). The shortest binding distance (r = 3.54 nm) and energy transfer efficiencies (E = 0.26) between donor (BSA) and acceptor (purpure-18-imide) were obtained by Forster's nonradiative energy transfer mechanism.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Algorithms
  • Animals
  • Cattle
  • Energy Transfer
  • Fluorescence*
  • Imides / chemical synthesis
  • Imides / chemistry*
  • Imides / metabolism
  • Kinetics
  • Models, Chemical
  • Molecular Structure
  • Porphyrins / chemical synthesis
  • Porphyrins / chemistry*
  • Protein Binding
  • Serum Albumin, Bovine / chemistry*
  • Serum Albumin, Bovine / metabolism
  • Spectrometry, Fluorescence
  • Spectrophotometry
  • Spectrophotometry, Ultraviolet

Substances

  • Imides
  • Porphyrins
  • purpure-18-imide
  • purpurin 18
  • Serum Albumin, Bovine