Purification and characterization of a functionally active Mycobacterium tuberculosis pyrroline-5-carboxylate reductase

Protein Expr Purif. 2006 Jan;45(1):241-8. doi: 10.1016/j.pep.2005.08.007. Epub 2005 Sep 13.

Abstract

Pyrroline-5-carboxylate reductase (P5CR) plays an important role in the survival of Mycobacterium tuberculosis and is related to virulence of this pathogen. RT-PCR analysis indicated that proC, encoding P5CR, was expressed at the transcriptional level cultured in vitro. The His-rMtP5CR with an N-terminal His-tag (His-rMtP5CR) was firstly purified in Escherichia coli and rMtP5CR was obtained by removal of the N-terminal fusion partner using enterokinase. His-rMtP5CR had considerable beta-pleated sheet analyzed by circular dichroism spectroscopy. The effect of pH, temperature, cations, denaturants, and detergents on the purified enzyme activity and stability was characterized. The N-terminal fusion partner was found to have very little effect on the biochemical properties of P5CR.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cells, Cultured
  • Circular Dichroism
  • Cloning, Molecular
  • DNA / genetics
  • Escherichia coli / cytology
  • Escherichia coli / genetics
  • Escherichia coli / metabolism
  • Gene Expression Regulation, Enzymologic
  • Hydrogen-Ion Concentration
  • Kinetics
  • Mycobacterium tuberculosis / enzymology*
  • Pyrroline Carboxylate Reductases / chemistry*
  • Pyrroline Carboxylate Reductases / genetics
  • Pyrroline Carboxylate Reductases / isolation & purification
  • RNA / genetics
  • Recombinant Fusion Proteins / chemistry
  • Recombinant Fusion Proteins / genetics
  • Recombinant Fusion Proteins / isolation & purification
  • Reverse Transcriptase Polymerase Chain Reaction / methods
  • Temperature

Substances

  • Recombinant Fusion Proteins
  • RNA
  • DNA
  • Pyrroline Carboxylate Reductases
  • pyrroline-5-carboxylate reductase, M tuberculosis