Methods for the detection of paxillin post-translational modifications and interacting proteins by mass spectrometry

J Proteome Res. 2005 Sep-Oct;4(5):1832-41. doi: 10.1021/pr0502020.

Abstract

Methods for the simultaneous identification of interacting proteins and post-translational modifications of the focal adhesion adapter protein, paxillin, are presented. The strategy includes (1) lower-level, transient transfection of FLAG-GFP-Paxillin into HEK293 cells, (2) incubation of cells with phosphatase inhibitors prior to lysis, (3) purification of paxillin by anti-FLAG immunoprecipitation, (4) analysis of peptides generated from on-beads digestion using LTQ-FT or LTQ-ETD mass spectrometry, and (5) enrichment of phosphopeptide methyl esters with IMAC. Using the above strategies, we identify 29 phosphorylation sites (19 novel and 10 previously reported) and a novel glycosylation site on Ser 74. Furthermore, with this method, we simultaneously detect 10 co-purifying proteins which are present in focal adhesion complexes. Extension of these methods to other substrates should facilitate generation of global phosphorylation maps and protein-protein interactions for any protein of interest.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Binding Sites
  • Cell Line
  • Chromatography, Ion Exchange
  • Electrons
  • Focal Adhesions
  • Glycosylation
  • Green Fluorescent Proteins / chemistry
  • Green Fluorescent Proteins / metabolism
  • Humans
  • Immunoprecipitation
  • Mass Spectrometry / methods*
  • Mice
  • Molecular Sequence Data
  • Paxillin / chemistry*
  • Peptides / chemistry
  • Phosphorylation
  • Plasmids / metabolism
  • Protein Binding
  • Protein Processing, Post-Translational
  • Serine / chemistry
  • Time Factors
  • Transfection
  • Trypsin / pharmacology
  • Vanadates / chemistry

Substances

  • Paxillin
  • Peptides
  • peroxovanadate
  • Green Fluorescent Proteins
  • Vanadates
  • Serine
  • Trypsin