Quantification of Ca(2+)-ATPases in porcine duodenum. Effects of 1,25(OH)2D3 deficiency

Biochim Biophys Acta. 1991 Jun 18;1065(2):177-84. doi: 10.1016/0005-2736(91)90228-z.

Abstract

Previous studies have identified a calmodulin-stimulated ATP-dependent Ca2+ pump as the major Ca2+ efflux pathway in enterocytes. Here, we developed methods to quantify the number of Ca2+ pumps in basolateral and intracellular membranes from porcine duodenum. By the use of a pig strain with a genetic defect in renal 1 alpha-hydroxylase, we were able to investigate the influence of 1,25(OH)2D3-deficiency on the number of Ca(2+)-ATPases in porcine duodenum. The amount of Ca(2+)-ATPase in isolated basolateral membranes was 5.5 +/- 0.7 micrograms/mg protein, while the Vmax of ATP-dependent Ca2+ transport into inside-out resealed basolateral membrane vesicles was 2.6 +/- 0.4 nmol/mg protein per min. From these data we estimated roughly about 95 x 10(3) plasma membrane Ca2+ pump sites per enterocyte. In addition, the amount of intracellular Ca(2+)-ATPase in microsomal fractions was 0.41 +/- 0.02 microgram/mg protein. Comparison of these parameters between control and rachitic animals showed that Ca2+ pump capacities in both basolateral membranes and microsomal fractions of porcine duodenum are not influenced by 1,25(OH)2D3-deficiency. In conclusion, stimulatory effects of 1,25(OH)2D3 on intestinal Ca2+ transport most likely result from specific effects on apical influx and facilitation of cytosolic Ca2+ diffusion by Ca(2+)-binding proteins and not from an increase in Ca2+ pumping capacity in basolateral membranes.

MeSH terms

  • Adenosine Triphosphate / pharmacology
  • Animals
  • Biological Transport, Active / drug effects
  • Blotting, Western
  • Calcitriol / deficiency*
  • Calcium / metabolism
  • Calcium Channels / metabolism
  • Calcium-Transporting ATPases / analysis
  • Calcium-Transporting ATPases / metabolism*
  • Calmodulin / metabolism
  • Cell Membrane / enzymology
  • Duodenum / enzymology*
  • Enzyme-Linked Immunosorbent Assay
  • Kinetics
  • Rickets / enzymology
  • Swine

Substances

  • Calcium Channels
  • Calmodulin
  • Adenosine Triphosphate
  • Calcium-Transporting ATPases
  • Calcitriol
  • Calcium