Direct enantio- and diastereoselective Mannich reactions of malonate and beta-keto esters with N-Boc and N-Cbz aldimines catalysed by a bifunctional cinchonine derivative

Chem Commun (Camb). 2006 Mar 21:(11):1191-3. doi: 10.1039/b515725k. Epub 2006 Feb 1.

Abstract

A highly enantioselective Mannich reaction between malonate esters and N-Boc and N-Cbz aldimines, catalysed by a bifunctional cinchonine derivative, has been developed; extension of this methodology to encompass the use of 2-substituted-1,3-dicarbonyl nucleophiles allows the formation of adjacent stereocentres, one of which is quaternary, in high relative and absolute stereocontrol.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Catalysis
  • Cinchona Alkaloids / chemistry*
  • Esters
  • Imines / chemistry*
  • Ketones / chemistry*
  • Malonates / chemistry*
  • Mannich Bases / chemistry
  • Models, Molecular
  • Molecular Structure
  • Stereoisomerism

Substances

  • Cinchona Alkaloids
  • Esters
  • Imines
  • Ketones
  • Malonates
  • Mannich Bases
  • malonic acid
  • cinchonine