A versatile and general one-pot method for synthesizing bis-spiroketal motifs

Org Lett. 2006 Apr 27;8(9):1945-8. doi: 10.1021/ol060558x.

Abstract

[reaction: see text] A versatile and general method for the biomimetic construction of [5,5,5]- and [6,5,6]-bis-spiroketals, starting from easily accessible furan nuclei, by means of a powerful one-pot singlet oxygen-mediated cascade sequence is reported.