The role of steric effects in the direct mutagenicity of N-acyloxy-N-alkoxyamides

Mutat Res. 2006 Jun 16;605(1-2):51-62. doi: 10.1016/j.mrgentox.2006.02.003. Epub 2006 May 15.

Abstract

Electrophilic N-acyloxy-N-alkoxyamides are mutagenic in Salmonella typhimurium TA100 without the need for S9 metabolic activation and they react with DNA at guanine-N7 at physiological pH. Since these are direct-acting mutagens, structural factors influence binding and reactivity with DNA. Mutagenicity in TA100 can be predicted by a QSAR incorporating hydrophobicity (logP), stability to substitution reactions at nitrogen (pK(a) of the leaving acid) and steric effects of para-aryl substituents (E(s)). A number of mutagens exhibit activities that deviate markedly from the predicted values and they fall into two classes: di-tert-butylated N-benzoyloxy-N-benzyloxybenzamides, which--because of their size--are most probably excluded from the major groove or are unable to achieve a transition state for reaction with DNA, and N-benzoyloxy-N-butoxyalkylamides with branching alpha-to the amide carbonyl, which are resistant to S(N)2 reactions at the amide nitrogen.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Benzamides / chemical synthesis
  • Benzamides / toxicity*
  • Binding Sites
  • DNA, Bacterial / chemistry*
  • Guanine / chemistry
  • Hydrogen-Ion Concentration
  • Hydrophobic and Hydrophilic Interactions
  • Mutagenicity Tests
  • Mutagens / chemical synthesis
  • Mutagens / toxicity*
  • Polyunsaturated Alkamides / chemical synthesis
  • Polyunsaturated Alkamides / toxicity*
  • Salmonella typhimurium / drug effects*
  • Salmonella typhimurium / genetics
  • Salmonella typhimurium / growth & development
  • Structure-Activity Relationship

Substances

  • Benzamides
  • DNA, Bacterial
  • Mutagens
  • Polyunsaturated Alkamides
  • Guanine