Mimicking the atmospheric OH-radical-mediated photooxidation of isoprene: formation of cloud-condensation nuclei polyols monitored by electrospray ionization mass spectrometry

Rapid Commun Mass Spectrom. 2006;20(14):2104-8. doi: 10.1002/rcm.2574.

Abstract

Recently, it has been proposed (M. Claeys et al., Science 2004; 303: 1173) that the atmospheric OH-radical-mediated photooxidation of isoprene is a source of two major secondary organic aerosol (SOA) components, that is, 2-methylthreitol and 2-methylerythritol. These diastereoisomeric tetrols, which were characterized for the first time in the fine size fraction (<2.5 microm aerodynamic diameter) of aerosols collected in the Amazon rain forest during the wet season, were proposed to enhance the capability of the aerosols to act as cloud-condensation nuclei. In the present study, we performed the oxidation of isoprene in aqueous solution under conditions that attempted to mimic atmospheric OH-radical-induced photooxidization, and monitored and characterized on-line the reaction products via electrospray ionization mass (and tandem mass) spectrometry in the negative ion mode. The results show that the reaction of isoprene with photo- or chemically generated hydroxyl radicals indeed yields 2-methyltetrols. Other polyols were also detected, and they may therefore be considered as plausible SOA components eventually formed in normal or more extreme OH-radical-mediated photooxidation of biogenic isoprene.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aerosols / chemistry
  • Air Pollutants / chemistry*
  • Air Pollutants / radiation effects
  • Atmosphere / chemistry
  • Butadienes / chemistry*
  • Butadienes / radiation effects
  • Environmental Monitoring / methods*
  • Erythritol / analysis
  • Hemiterpenes / chemistry*
  • Hemiterpenes / radiation effects
  • Hydroxyl Radical / chemistry*
  • Hydroxyl Radical / radiation effects
  • Oxidation-Reduction
  • Particle Size
  • Pentanes / chemistry*
  • Pentanes / radiation effects
  • Photochemistry
  • Polymers / analysis*
  • Spectrometry, Mass, Electrospray Ionization / methods*
  • Stereoisomerism
  • Sugar Alcohols / analysis

Substances

  • Aerosols
  • Air Pollutants
  • Butadienes
  • Hemiterpenes
  • Pentanes
  • Polymers
  • Sugar Alcohols
  • polyol
  • isoprene
  • Hydroxyl Radical
  • threitol
  • Erythritol