Composite-hydroxide-mediated approach for the synthesis of nanostructures of complex functional-oxides

Nano Lett. 2006 Jul;6(7):1535-40. doi: 10.1021/nl061253e.

Abstract

We demonstrate a generic approach for the synthesis of single-crystal complex oxide nanostructures of various structure types, such as perovskites, spinels, monoclinic, corundum, CaF(2) structured, tetragonal, and even metal hydroxides. The method is based on a reaction between a metallic salt and a metallic oxide in a solution of composite-hydroxide eutectic at approximately 200 degrees C and normal atmosphere without using an organic dispersant or capping agent. The synthesis technique is cost-effective, one-step, easy to control, and is performed at low temperature and normal atomospheric pressure. The technique can be expanded to many material systems, and it provides a general, simple, convenient, and innovative strategy for the synthesis of nanostructures of complex oxides with important scientific and technological applications in ferroelectricity, ferromagnetism, colossal magnetoresistance, fuel cell, optics, and more.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Calcium Compounds / chemical synthesis
  • Calcium Compounds / chemistry
  • Hydroxides / chemistry*
  • Macromolecular Substances / chemical synthesis
  • Macromolecular Substances / chemistry
  • Nanostructures / chemistry*
  • Oxides / chemical synthesis
  • Oxides / chemistry*
  • Titanium / chemistry

Substances

  • Calcium Compounds
  • Hydroxides
  • Macromolecular Substances
  • Oxides
  • perovskite
  • Titanium