Synthesis, DNA-binding and photocleavage studies of ruthenium(II) complex with 2-(3'-phenoxyphenyl)imidazo[4,5-f][1,10]phenanthroline

J Inorg Biochem. 2007 Jan;101(1):56-63. doi: 10.1016/j.jinorgbio.2006.08.006. Epub 2006 Aug 30.

Abstract

A new polypyridyl ligand MPPIP {MPPIP=2-(3'-phenoxyphenyl)imidazo[4,5-f]-[1,10]phenanthroline} and its ruthenium(II) complexes, [Ru(bpy)(2)MPPIP](2+) (1) (bpy=2,2'-bipyridine) and [Ru(phen)(2)MPPIP](2+) (2) (phen=1,10-phenanthroline) have been synthesized and characterized. The binding of the two complexes to calf thymus DNA (CT-DNA) has been investigated with spectrophotometric methods, viscosity measurements, as well as equilibrium dialysis and circular dichroism spectroscopy. The results suggest that both complexes bind to CT-DNA through intercalation, and enantioselectively interact with CT-DNA in a way. However, complex 2 is a much better candidate as an enantioselective binder to CT-DNA than complex 1. When irradiated at 365nm, both complexes have also been found to promote the photocleavage of plasmid pBR322 DNA.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Imidazoles / chemical synthesis*
  • Imidazoles / chemistry
  • Imidazoles / pharmacology
  • Phenanthrolines / chemical synthesis*
  • Phenanthrolines / chemistry
  • Phenanthrolines / pharmacology
  • Photochemistry
  • Ruthenium / chemistry*
  • Spectrometry, Mass, Electrospray Ionization
  • Spectrometry, Mass, Fast Atom Bombardment
  • Spectrophotometry, Ultraviolet

Substances

  • 2-(3'-phenoxyphenyl)imidazo(4,5-f)(1,10)phenanthroline
  • Imidazoles
  • Phenanthrolines
  • Ruthenium