Controllable synthesis of vertically aligned ZnO nanorod arrays in aqueous solution

J Nanosci Nanotechnol. 2006 Jul;6(7):2062-6. doi: 10.1166/jnn.2006.354.

Abstract

High-density well-aligned ZnO nanorod array was successfully synthesized on a large-area magnetron sputtering deposited Al doped ZnO film-coated Si (AZO/Si) substrate via a convenient solution method. X-ray diffraction and scanning electron microscopy show that the nanorods are well-oriented perpendicular to the substrate. The influences of the reaction temperature, time, on the size and shapes of the as-prepared ZnO nanorods (ZNs) samples have been studied. The length and diameter of the nanorods became bigger when a longer reaction time was used. When the temperature is elevated to 130 degrees C, a new conical ZNs was synthesized. Room-temperature photoluminescence (PL) spectra of all the ZnO products showed a strong ultraviolet (UV) emission. The photoluminescence from free excitons of the ZNs synthesized at higher temperature reflects the high purity and nearly defect free structure of nanorods. The well-aligned feature of the nanorod array is attributed to the nanorods' epitaxial growth from the AZO films.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Crystallization / methods*
  • Macromolecular Substances / chemistry
  • Materials Testing
  • Molecular Conformation
  • Nanostructures / chemistry*
  • Nanostructures / ultrastructure*
  • Nanotechnology / methods*
  • Particle Size
  • Solutions
  • Surface Properties
  • Temperature
  • Water / chemistry*
  • Zinc Oxide / chemistry*

Substances

  • Macromolecular Substances
  • Solutions
  • Water
  • Zinc Oxide