Synthetic cryptolepine inhibits DNA binding of NF-kappaB

Bioorg Med Chem. 2007 Jan 1;15(1):43-9. doi: 10.1016/j.bmc.2006.10.018. Epub 2006 Oct 24.

Abstract

The alkaloid cryptolepine is thought to mediate the anti-inflammatory effects of the climbing shrub, Cryptolepis sanguinoleta. The underlying mechanism of action, however, is largely unknown. In the present study, we show that the synthetic cryptolepine-hydrochloride (2.5-10microM) dose-dependently inhibits lipopolysaccharide (LPS)-induced nitric oxide production in the murine macrophage cell line RAW 264.7. We furthermore demonstrate a strong inhibition of nuclear factor (NF)-kappaB, a transcription factor primarily involved in inflammatory and immune responses, by cryptolepine (2.5-10microM) using a luciferase reporter gene assay in human HEK 293 cells. Examining the individual steps of NF-kappaB activation in the presence of cryptolepine we could exclude an inhibitory effect on degradation of IkappaB or nuclear translocation of NF-kappaB by the alkaloid. However, EMSA of nuclear extracts from LPS-activated RAW cells revealed reduced DNA binding activity of NF-kappaB by cryptolepine in vivo and in vitro. This indicates that cryptolepine may exhibit its anti-inflammatory action by blocking DNA binding of activated NF-kappaB and thus transcription of NF-kappaB-regulated proinflammatory proteins.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkaloids / chemical synthesis
  • Alkaloids / pharmacology*
  • Animals
  • Anti-Inflammatory Agents / chemical synthesis
  • Anti-Inflammatory Agents / pharmacology*
  • Binding Sites
  • Binding, Competitive / drug effects
  • Cell Line
  • Cells, Cultured
  • Cryptolepis / chemistry
  • DNA / drug effects*
  • Dose-Response Relationship, Drug
  • Drug Evaluation, Preclinical
  • Humans
  • Indole Alkaloids
  • Indoles / chemical synthesis
  • Indoles / pharmacology*
  • Lipopolysaccharides / antagonists & inhibitors
  • Macrophages / cytology
  • Macrophages / drug effects*
  • Macrophages / metabolism
  • Mice
  • NF-kappa B / antagonists & inhibitors*
  • NF-kappa B / genetics
  • Nitric Oxide / antagonists & inhibitors
  • Nitric Oxide / biosynthesis
  • Quinolines / chemical synthesis
  • Quinolines / pharmacology*
  • Structure-Activity Relationship
  • Transcription, Genetic / drug effects

Substances

  • Alkaloids
  • Anti-Inflammatory Agents
  • Indole Alkaloids
  • Indoles
  • Lipopolysaccharides
  • NF-kappa B
  • Quinolines
  • Nitric Oxide
  • cryptolepine
  • DNA