1H and 13C NMR spectral assignment of alkyl and polyamine-linked bis(2-thioxo-[1,3,5]-thiadiazinan-3-yl) carboxylic acids

Dolores Molero; Julieta Coro; Rolando Pérez; Margarita Suárez; Roberto Martínez-Alvarez; Antonio Herrera; Nazario Martín

doi:10.1002/mrc.1921

1H and 13C NMR spectral assignment of alkyl and polyamine-linked bis(2-thioxo-[1,3,5]-thiadiazinan-3-yl) carboxylic acids

Magn Reson Chem. 2007 Jan;45(1):93-8. doi: 10.1002/mrc.1921.

Authors

Dolores Molero¹, Julieta Coro, Rolando Pérez, Margarita Suárez, Roberto Martínez-Alvarez, Antonio Herrera, Nazario Martín

Affiliation

¹ CAI-RMN, Universidad Complutense, E-28040 Madrid, Spain.

PMID: 17103485
DOI: 10.1002/mrc.1921

Abstract

The 1H and 13C NMR spectroscopic data for alkyl and polyamine-linked bis(2-thioxo-[1,3,5]thiadiazinan-3-yl) carboxylic acids, prepared from alkyl diamines and N4-(benzyl) spermidine have been fully assigned by combination of one- and two-dimensional experiments (DEPT, HMBC, HMQC, COSY).