Development and validation of a high-throughput screen for inhibitors of SARS CoV and its application in screening of a 100,000-compound library

J Biomol Screen. 2007 Feb;12(1):33-40. doi: 10.1177/1087057106296688. Epub 2006 Dec 22.

Abstract

The authors have developed a high-throughput screen (HTS) that allows for the identification of potential inhibitors of the severe acute respiratory syndrome coronavirus (SARS CoV) from large compound libraries. The luminescent-based assay measures the inhibition of SARS CoV-induced cytopathic effect (CPE) in Vero E6 cells. The assay was validated in 96-well plates in a BSL3 containment facility. The assay is sensitive and robust, with Z values > 0.6, signal to background (S/B) > 16, and signal to noise (S/N) > 3. The assay was further validated with 2 different diversity sets of compounds against the SARS CoV. The "hit" rate for both libraries was approximately 0.01%. The validated HTS assay was then employed to screen a 100,000-compound library against SARS CoV. The hit rate for the library in a single-dose format was determined to be approximately 0.8%. Screening of the 3 libraries resulted in the identification of several novel compounds that effectively inhibited the CPE of SARS CoV in vitro-compounds which will serve as excellent lead candidates for further evaluation. At a 10-microM concentration, 3 compounds with selective indexes (SI50) of > 53 were discovered.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Animals
  • Antiviral Agents / analysis*
  • Antiviral Agents / chemistry
  • Antiviral Agents / pharmacology*
  • Cell Count
  • Chlorocebus aethiops
  • Combinatorial Chemistry Techniques / methods*
  • Dimethyl Sulfoxide
  • Drug Evaluation, Preclinical
  • Endpoint Determination
  • Inhibitory Concentration 50
  • Luminescence
  • Reproducibility of Results
  • Severe acute respiratory syndrome-related coronavirus / drug effects*
  • Vero Cells

Substances

  • Antiviral Agents
  • Dimethyl Sulfoxide